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Psychiatry 9 , 7682 (2014)

Despite this substantial research history, DSIP has not achieved widespread clinical acceptance or regulatory approval in major markets, reflecting challenges including inconsistent clinical results, unclear mechanisms, difficulty in establishing optimal dosing, route, and timing protocols, and competition from better-characterized sleep and stress medications

Peptide samples were analyzed with a high-energy collisional dissociation (HCD) fragmentation method with normalized collision energy at 25 and 41, acquiring one Orbitrap survey scan in the mass range of m/z 3002000 followed by MS/MS of the three most intense ions in the Orbitrap (R7500)

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